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This new edition provides an in-depth introduction to the theories and applications of the powder diffraction method for structure determination. The emphasis is placed on powder diffraction data collected using conventional x-ray sources, which remain primary tools for thousands of researchers and students in their daily experimental work. The book is divided into two parts: chapters one though fifteen give essential theoretical background, while chapters sixteen through twenty-five guide the reader through practical aspects of extracting structural information from powder data. Fundamentals of Powder Diffraction and Structural Characterization of Materials, Second Edition is suited for undergraduate and graduate students and practitioners from materials science, solid-state chemistry, physics, geology, and literally any other science or engineering background, who demand structural information at the atomic resolution using the powder diffraction method. Key features of the second edition: The book requires no prior knowledge of the subject, but is comprehensive and detailed making it useful for both the novice and experienced user of the powder diffraction method. While developed as a text to teach students, the book is also a reference for academic and industrial researchers using the powder diffraction method in their daily work. Major revisions include expanded treatment of non-crystallographic symmetry brief introductions to the total scattering analysis and non-ambient powder diffractometry basics of quantitative analysis using the Rietveld method, including determination of amorphous content addition of a difficult pseudo-symmetric indexing case expanded coverage of direct space structure solution techniques an introduction to the mechanism of constraints, restraints and rigid bodies and a new example of structure solution of a pharmaceutical compound additional problems to help in assessment of students' progress. The book is supplemented by online content, including color figures, powder diffraction data, examples, and web links.

Fundamentals of Crystalline State and Crystal Lattice 1
Finite Symmetry Elements and Crystallographic Point Groups 17
Infinite Symmetry Elements and Crystallographic Space Groups 51
Formalization of Symmetry 77
Nonconventional Symmetry 97
Properties, Sources, and Detection of Radiation 107
Fundamentals of Diffraction 133
The Powder diffraction Pattern 151
Structure Factor 203
Solving the Crystal Structure 239
Powder Diffractometry 263
Collecting Quality Powder Diffraction Data 301
Preliminary Data Processing and Phase Analysis 347
Determination and Refinement of the Unit Cell 407
Solving Crystal Structure from Powder Diffraction Data 497
Crystal Structure of LaNi4.85Sn0.15 547
Crystal Structure of CeRhGe3 579
Crystal Structure of Nd5Si4 603
Empirical Methods of Solving Crystal Structures 611
Crystal Structure of NiMnO2(OH) 633
Crystal Structure of tmaV3O7 655
Crystal Structure of ma2Mo7O22 669
Crystal Structure of Mn7(OH)3(VO4)4 679
Crystal Structure of FePO4 691
Crystal Structure of Acetaminophen, C8H9NO2 703
Index 729
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